OUTROS EQUIPAMENTOS DE MEDIÇÃO DE PARTÍCULAS
Laser Particle Sizer
ANALYSETTE 22
NeXT MicroEach measuring unit ANALYSETTE 22 NeXT Micro with USB-Interface, is delivered with a computer* with already installed software MaS control, monitor, keyboard and mouse.
*without computer hardware for deliveries to CIS countries
Choose exactly according to your needs
The ANALYSETTE 22 NeXT Micro is developed according to a smart modular concept. You only buy what you really need. Therefore you can flexibly grow with your sizing tasks. Modules can be added to at any time, and we are constantly developing the portfolio. We offer a dry and wet dispersion unit. In addition, you can choose an ultrasonic box, a pH probe, conversion kits for extreme chemical resistance, exhaust systems, compressor, reference materials, certificates and spare parts.
For representative sample division - the foundation of any precise analysis - we recommend the
Rotary Cone Sample Divider LABORETTE 27
Dry dispersion unit and accessories
Dry dispersion is especially suited for not too fine, free-flowing materials, which react in water or other liquids. For sample volumes from less than 1 cm3 up to approx. 300 cm3.
An external exhaust system is necessary to ensure automatic sample exhaust during the measurement. When the measurement is completed it can also be easily used to manually clean the feeder. Two different exhaust systems are available and can be ordered as a FRITSCH accessory together with the instrument.
Dry dispersion unit and accessories
Automatic dry dispersion unit for sample volumes from less than 1 cm3 up to approx. 300 cm3 - especially suited for not too fine, free-flowing materials, which react in water or other liquids.
The ultra-compact dry dispersion unit has a height-adjustable funnel and stirrer made of stainless steel ensuring optimum sample feeding adapted to the respective sample material. All parts that come into contact with the sample can be easily dismantled - thus guaranteeing absolutely fast and easy cleaning. Also the measuring cell of the ANALYSETTE 22 NeXT can be opened without tools by means of an eccentric lock. Its cleaning is quite convenient by an easily re-insertable outer seal. And also the exchange of the measuring cell glasses can be done any time completely uncomplicated.
In dry measurement the sample material is transported with a vibratory feeder through the intake funnel into the dry measuring cell, where it falls directly into a Venturi nozzle operating with an adjustable flow of compressed air. Upon passing through the nozzle, agglomerates are broken up and the measurement of the particle size dispersion in the laser beam takes place directly afterwards.
for practical storing of the wet resp. dry measuring cell
The exhaust system, dust category "M" according to DIN EN 60335-2-69 for 230 V/1~, 50/60 Hz, 1600 Watt is versatile:
For combination with the high performance and small volume cyclones.
To operate the FRITSCH Cyclones you need an exhaust system. The strong airflow ensures simple feeding, increases throughput, and reduces the thermal load of the samples. The high performance and small volume Cyclone separator can be combined with Universal Cutting Mills PULVERISETTE 19, the Variable Speed Rotor Mill PULVERISETTE 14 premium line and classic line. The small volume cyclone can also be combined with the Variable Speed Rotor Mill PULVERISETE 14 premium line and classic line even for passive utilisation – without sample exhaust.
The high-performance cyclone is ideal for combination with the Universal Cutting Mills PULVERISETTE 19 large, the Cross Beater Mill PULVERISETTE 16 and the Disk Mill PULVERISETTE 13 premium line for optimal sample extraction and for comminution of larger quantities.
For cooling of the Variable Speed Rotor Mill PULVERISETTE 14 premium line
By connecting the exhaust system with the connecting piece order no. 14.4214.00, the cooling of the mill can easily be enhanced.
For connecting to Disk Mill PULVERISETTE 13 premium line
The exhaust is simply connected to the PULVERISETTE 13 premium line and operated via a start and stop button on the instrument – for dust free comminution.
For connecting to the Jaw Crusher PULVERISETTE 1, Modell I + II classic line
Simply connect the exhaust system to the integrated connection of the PULVERISETTE 1. Fine dust arising during comminution is automatically removed. The exhaust system is also very useful when cleaning the grinding parts.
For connecting to the Disk Mill PULVERISETTE 13 classic line
The exhaust system can be easily connected to the PULVERISETTE 13 classic line. Fine dust arising during comminution is automatically removed. The exhaust system is also very useful when cleaning the grinding parts.
For exhaustion of the sample during dry measurement with the Laser Particle Sizers ANALYSETTE 22 NeXT
An exhaust system is necessary to ensure automatic sample exhaustion during dry measurement. When the measurement is completed it can also be easily used to manually clean the feeder.
Please note that the exhaust system article no. 43.9070.00, is not equipped with a fine filter and therefore dust may escape. Please consider the valid occupational health and safety regulations. This exhaust system is mostly recommended for dust-free grinding and the vacuuming of during the process developing fine dust in the upper part of the grinding chamber and for the cleaning of the grinding parts.
For vacuuming of the sample during dry measurement with the Laser Particle Sizers ANALYSETTE 22 NeXT, we recommended we recommend the exhaust system article no. 43.9060.00, which is equipped with a hose and an ultra-fine filter of dust class "H" according to DIN EN 60335-2-69, so that the escape of fine dust is reduced.
For 230 V/1~, 50-60 Hz, 1000 Watt
This exhaust system is equipped with a hose and ultra-fine filter of the dust category "H" according to DIN EN 60335-2-69, so the escape of fine dust is avoided. This exhaust system is especially recommended for the vacuuming of the sample during the dry measurement with the Laser Particle Sizers ANALYSETTE 22 NeXT.
Another exhaust system is offered; please refer to article no. 43.9070.00. Please note that this exhaust system is not equipped with a fine filter and therefore dust may escape. Please consider the valid occupational health and safety regulations. This exhaust system is mostly recommended for dust-free grinding and the vacuuming of during the process developing fine dust in the upper part of the grinding chamber and for the cleaning of the grinding parts.
For 230 V/1~, 108 l/min oil-free
For the operation of the dry dispersion unit if no oil-, water- and particle-free supply of compressed air with a pressure of at least 5 bar and an air volume of at least 125 l/min is available.
Spare parts for exhaust systems
1 pack = 5 pieces
One pack is included in the scope of delivery of the exhaust system (article No. 43.9070.00).
These fleece filter bags should be used for the vacuuming off of fine, dry materials.
For the vacuuming off of coarse, wet materials are plastic bags available (article no. 43.9052.00).
1 pack = 5 pieces
One pack is included in the order of the exhaust system (article No. 43.9070.00).
These plastic bags should be used for the vacuuming off of coarse, wet materials.
For the vacuuming off of fine, dry materials are paper filter bags available (article no. 43.9055.00).
1 Pack = 3 pieces
One pack is included in the order of the exhaust system (article no. 43.9060.00)
1 piece is included in the order of the exhaust system (article no. 43.9060.00).
Wet dispersion units and accessories
For most samples, wet dispersion represents the ideal method of preparation for particle size measurement. For this reason, we offer a quite powerful, flexible and modular wet dispersion system.
A pH probe is offered for continuous monitoring of the pH value of the dispersion liquid - covers fluctuations much more effectively than the zeta potential.
For working with extremely aggressive chemical dispersion liquids, order the wet dispersion unit with the conversion kit Extended for extreme chemical resistance.
Wet Dispersion Unit and accessories
Automatic wet dispersion unit, volume 150-500 ml, suitable for most samples.
A powerful centrifugal pump with individually adjustable speed ensures stable measuring in the dispersion unit of the ANALYSETTE 22 NeXT. It also transports heavy particles and facilitates a fast and uniform distribution of the sample material in the entire circulation system. Standard programs for simple operation, freely programmable dispersion process, an especially fast and efficient automatic cleaning and many other advantages also simplify your work. And ensure the quality of your measuring results.
Read details about our Wet Dispersion Unit here
for covering the sample bath of the wet dispersion unit.
The cover provides safe splash protection during filling, dispersion and rinsing.
for filling the wet dispersion unit if no suitable media connection is available
for practical storing of the wet resp. dry measuring cell
for simple, continuous monitoring of the pH value of the dispersion liquid
The new pH sensor is installed as a module in the dispersion bath and connected to the Laser Particle Sizers ANALYSETTE 22 NeXT. It continuously measures the pH value during the measurement and automatically transfers the determined values to the software for documentation.
This method covers fluctuations much more effectively than the zeta potential and offers many advantages, especially in the area of research and development.
The pH value is much broader, especially with measurements in the field of nano-suspensions. Its monitoring provides valuable information about how and when a chemically inert material, for example, reacts to alkalis, depending on the environment. If the curve is unstable and varies during measurement, the pH value helps with stabilization and interpretation. The pH measurement process introduced by FRITSCH enables to observe these values precisely. The detection of agglomeration or aggregation is also much easier.
for wet dispersion unit consisting of seals, flow plate and hoses
The conversion kit Extended for extreme chemical resistance consists of seals and flow plate made of FFKM – inside of the hoses are made of FEP.
If you are working with extremely aggressive chemical dispersion liquids, you can order the wet dispersion unit with this conversion kit for extreme chemical resistance.
If you already have an instrument, you can order the conversion kit separately to retrofit your equipment.
A list providing an overview of chemicals can be downloaded here:
List of suitable chemicals
for wet dispersion unit in combination with ultrasonic box consisting of seals, flow plate and hoses
The conversion kit Extended for extreme chemical resistance consists of seals and flow plate made of FFKM – inside of the hoses are made of FEP.
If you are working with extremely aggressive chemical dispersion liquids, you can order the wet dispersion unit with this conversion kit for extreme chemical resistance.
If you already have an instrument, you can order the conversion kit separately to retrofit your equipment.
A list providing an overview of chemicals can be downloaded here:
List of suitable chemicals
Oil Dispersion Unit
The wet dispersion unit for viscous liquids for automatic dispersion volume (150-500 ml) is now available and can be ordered under article no. 22.9400.00. It's suitable for dispersion liquids with a dynamic viscosity of up to approx. 75 mPas, such as sunflower oil. Therefore it can be used for wet dispersion and measuring for example of chocolate.
Ultrasonic Boxes and accessories
Our powerful ultrasonic box is simply inserted into the sample circulation system. We offer two models with different voltages.
Ultrasonic Boxes and accessories
for dispersion with ultrasonic with max. 50 Watt ultrasonic output,
variably adjustable for 200-240 V/1~, 50-60 Hz, 60 Watt
If you measure sample material frequently that tends to agglomerate, you can equip your ANALYSETTE additionally with a powerful ultrasonic box which is simply inserted into the sample circulation system. It allows for an even finer adjustment of the wet dispersion to the respective sample material and operates extremely quietly with less than 45 dB.
All parts inside the ultrasonic box, which come into contact with the dispersion medium are made of high-quality stainless steel 316Land FFKM.
for dispersion with ultrasonic with max. 50 Watt ultrasonic output,
variably adjustable for 100-120 V/1~, 50-60 Hz, 60 Watt
If you measure sample material frequently that tends to agglomerate, you can equip your ANALYSETTE additionally with a powerful ultrasonic box which is simply inserted into the sample circulation system. It allows for an even finer adjustment of the wet dispersion to the respective sample material and operates extremely quietly with less than 45 dB.
All parts inside the ultrasonic box, which come into contact with the dispersion medium are made of high-quality stainless steel 316L and FFKM.
Reference materials and certificates
To inspect your Particle Sizer to ensure proper function, various reference materials can be used for a reliable check of the system.
The reference materials offered by FRITSCH are delivered along with precise dispersion and measurement instructions and are accompanied by a certificate containing the upper and lower limits of the expected particle sizes. These limit values were determined using an internationally recognised process (NIST-traceable).
Certified reference materials (NIST-traceable) for performance verification according to ISO 13320
Test powder for dry dispersion, 50 - 350 µm (box with 10 single-shots 5 g) certified reference material for performance verification of the FRITSCH Laser Particle Sizers ANALYSETTE 22, which are used for dry dispersion and for calibration according to ISO 13320 in regard to repeatability and reproducibility.
The test powder for dry dispersion is delivered in a box with 10 single-shots 5 g.
Also a test powder for wet dispersion, as well as test suspensions for the inspection of the measurement precision are offered.
Box with FRITSCH-test powder F-500 for 0.5 - 50 μm (50 g), 3 single-shots test powder 10 - 100 μm (0.5 g), 3 single-shots test suspension nano (approx. 200 nm) for system check (5 ml), 3 single-shots test suspension1 μm for system check (5 ml), 3 single-shots test suspension 10 μm forsystem check (5 ml).
Test powder for wet dispersion, 10 - 100 µm (Box with 10 single-shots 0.5 g), certified reference material for performance verification of the FRITSCH Laser Particle Sizers ANALYSETTE 22, which are used for wet dispersion and for calibration according to ISO 13320 in regard to repeatability and reproducibility.
The test powder for wet dispersion is delivered in a box with 10 single-shots 0.5 g.
Also test suspensions for the inspection of the measurement precision are offered.
Test suspension nano (approx. 200 nm) for system check (box with 10 single-shots 5 ml) for the inspection of the measurement precision of the FRITSCH Laser Particle Sizers ANALYSETTE 22, which are used for wet dispersion.
The test suspension nano for system check for wet dispersion is delivered in a box with 10 single-shots 5 ml.
Additional test suspensions for inspection of the measurement precision, as well as test powders for the calibration of the Laser Particle Sizers ANALYSETTE 22 according to ISO 13320 in regard to repeatability and reproducibility are also offered.
Test suspension 1 µm for system check (Box with 10 single-shots 5 ml) for inspection of the measurement precision of the FRITSCH Laser Particle Sizers ANALYSETTE 22, which are used for wet dispersion.
The test suspension 1 µm for system check for wet dispersion is delivered in a box with 10 single-shots 5 ml.
Additional test suspensions for inspection of the measurement precision as well as test powders for the calibration of the Laser Particle Sizers ANALYETTE 22 according to ISO 13320 in regard to repeatability and reproducibility are also offered.
Test suspension 10 µm for system check (Box with 10 single-shots 5 ml) for inspection of the measurement precision of the FRITSCH Laser Particle Sizers ANALYSETTE 22, which are used for wet dispersion.
The test suspension 10 µm for system check for wet dispersion is delivered in a box with 10 single-shots 5 ml.
Additional test suspensions for inspection of the measurement precision, as well as test powders for the calibration of the Laser Particle Sizers ANALYSETTE 22 according to ISO 13320 in regard to repeatability and reproducibility are also offered.
FRITSCH reference materials according to ISO 13320
For calibration of the Laser Particle Sizers ANALYSETTE 22 for dry dispersion within the framework of a test equipment monitoring system as per ISO 13320.
The cost-efficient alternative (non-certified reference materials) for regular inspection of your Laser Particle Sizers ANALYSETTE 22.
The FRITSCH-test powder F-70, 10 - 600 µm is delivered in a handy 150 g bottle.
For calibration of the Laser Particle Sizers ANALYSETTE 22 for wet dispersion within the framework of a test equipment monitoring system as per ISO 13320.
The cost-efficient alternative (non-certified reference materials) for regular inspection of your Laser Particle Sizers ANALYSETTE 22.
The FRITSCH-test powder F-500, 0.5 - 50 µm is delivered in a handy 50 g bottle.
Certification
Set of IQ/OQ blank forms (questionnaire format – implementation by customer – standards not
included).
Certificates for testing according to ISO 13320 on request.
Spare parts for dry and wet dispersion unit
Spare parts like measuring cell glasses for dry and wet dispersion unit.
Hoses and seals on request.
Replacement measuring cell glasses
Replacement dry measuring cell glas cpl. 4.65 mm for inserting into the flow measuring cell of the dry dispersion unit 22.9300.00.
Easy cleaning and exchange of the measuring cell
The measuring cell for the ANALYSETTE 22 NeXT is simply inserted from the front into the instrument as a practical cartridge and can be opened without tools with an eccentric lock. Its cleaning is quite convenient by an easily re-insertable outer seal. And also the exchange of the measuring cell glasses can be done any time completely uncomplicated.
Replacement flow measuring cell glass 4 mm for inserting into the flow measuring cell of the wet dispersion unit 22.9200.00.
Easy cleaning and exchange of the measuring cell
The measuring cell for the ANALYSETTE 22 NeXT is simply inserted from the front into the instrument as a practical cartridge and can be opened without tools with an eccentric lock. Its cleaning is quite convenient by an easily re-insertable outer seal. And also the exchange of the measuring cell glasses can be done any time completely uncomplicated.
